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Beilstein J. Org. Chem. 2017, 13, 1222–1229, doi:10.3762/bjoc.13.121
Graphical Abstract
Scheme 1: Overview of the hydrolysis–reductive amination procedure to produce primary glycamine 3 and byprodu...
Scheme 2: Overview of synthetic procedures, yields and specific rotation of glycamines 3, 7, 8, epi-8, 9 and ...
Figure 1: 1H NMR spectrum comparison of glycamines at 600 MHz, D2O, pH 4.0. Compound 3 in green, 7 in blue, 8...
Figure 2: Comparison of the ring distortion among glycamines 7, 9 and 13, and (+)-muscarine 14. Torsion angle...